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Beilstein J. Org. Chem. 2010, 6, No. 61, doi:10.3762/bjoc.6.61
Graphical Abstract
Figure 1: Antimalaria active natural artemisinin 1 and the spirobicyclic 1,2,4-trioxane derivative 2 show the...
Scheme 1: Singlet oxygen ene reaction of methyl 4-hydroxytiglate (3) and mesitylol (6) under solid-phase cond...
Scheme 2: 1,2,4-trioxane 9c and bis-trioxane 8a,b formation from the bifunctional cyclohexa-1,4-dione.
Figure 2: Structure of the spirobicyclic trioxane 5c in the crystal.
Scheme 3: BF3-catalyzed acetalization of hydroperoxide 4 with benzaldehyde derivatives.
Figure 3: Structure of the 3-arylated trioxane 10b in the crystal.
Figure 4: Structure of the p-bromophenyl derivative 10d in the crystal lattice (disordered water molecules in...
Figure 5: Numbering of 3-aryl-1,2,4-trioxanes 10 and relevant bonds; structure of artemether (AM).